1.) Count the distinct peaks in a spectra to determine the number of unique Hydrogen environments.
2.) Make an educated guess regarding Chemical Shifts (shielding/deshielding of electrons) and the relative upfield/downfield placement on the spectra. In 1H NMR Spectra the electromagnetic range is in PPM between 0-70
3.) Check for relative peak height. The relative peak heights are directly proportional the number of Hydrogens a molecule has.
4.) Determine peak splitting. The splitting of a peak into multiplets or a single peak shows the affects of neighboring hydrogens, thus helping to identify possible molecular structures.
5.) Cross reference with other experimental methods.
Saturday, January 17, 2009
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